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Mechanical and microstructural investigations of tungsten and doped tungsten materials produced via powder injection molding

机译:通过粉末注射成型生产的钨和掺杂钨材料的机械和微观结构研究

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摘要

The physical properties of tungsten such as the high melting point of 3420°C, the high strength and thermal conductivity, the low thermal expansion and low erosion rate make this material attractive as a plasma facing material. However, the manufacturing of such tungsten parts by mechanical machining such as milling and turning is extremely costly and time intensive because this material is very hard and brittle.Powder Injection Molding (PIM) as special process allows the mass production of components, the joining of different materials without brazing and the creation of composite and prototype materials, and is an ideal tool for scientific investigations.This contribution describes the characterization and analyses of prototype materials produced via PIM. The investigation of the pure tungsten and oxide or carbide doped tungsten materials comprises the microstructure examination, element allocation, texture analyses, and mechanical testing via four-point bend (4-PB). Furthermore, the different materials were characterized by high heat flux (HHF) tests applying transient thermal loads at different base temperatures to address thermal shock and thermal fatigue performance. Additionally, HHF investigations provide information about the thermo-mechanical behavior to extreme steady state thermal loading and measurements of the thermal conductivity as well as oxidation tests were done.Post mortem analyses are performed quantifying and qualifying the occurring damage with respect to reference tungsten grades by metallographic and microscopical means.
机译:钨的物理特性(如3420°C的高熔点,高强度和导热性,低热膨胀性和低腐蚀率)使该材料具有吸引力,可作为面向等离子体的材料。但是,通过机械加工(例如铣削和车削)制造此类钨零件非常昂贵且耗时,因为这种材料非常坚硬且易碎。粉末注射成型(PIM)作为特殊工艺可以实现零件的批量生产,无需钎焊即可创建不同的材料,也无需创建复合材料和原型材料,是进行科学研究的理想工具。此文稿描述了通过PIM生产的原型材料的特性和分析。纯钨和氧化物或碳化钨掺杂的钨材料的研究包括微观结构检查,元素分配,织构分析以及通过四点弯曲(4-PB)进行的机械测试。此外,不同的材料通过高热通量(HHF)测试来表征,这些测试在不同的基础温度下施加了瞬态热负荷,以解决热冲击和热疲劳性能。此外,HHF研究还提供了有关极端稳态热负荷下的热机械行为的信息,并进行了热导率的测量和氧化测试。进行了事后分析,以量化和鉴定相对于参考钨品位的发生损坏金相和显微手段。

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